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Beilstein J. Org. Chem. 2015, 11, 583–588, doi:10.3762/bjoc.11.64
Graphical Abstract
Scheme 1: (i) CAN, wet silica, KBr, CH2Cl2/CH3CN (1:1), rt, 30 min; (ii) a. NaOAc, Ac2O, 140 °C, 3 h; b. K2CO3...
Figure 1: Single X-ray crystal structure of hemithioacetal 3a.
Scheme 2: Proposed reaction sequence for the synthesis of a mixture of carbaldehydes 5a and 5a’ using Raney n...
Scheme 3: K2CO3 (catalytic amount), MeOH, rt, 30 min.